NPLB14027U Analytical Chemistry
BSc Programme in Chemistry
BSc Programme in Natural Resources
BSc Programme in Biology-Biotechnology
BSc Programme in Food and Nutrition
MSc Programme in Food Science and Technology
MSc Programme in Biology-Biotechnology
The course topics include: An introduction to analytical
chemistry: choice of analytical methodology, sampling, sample
preparation, chemical analysis, tools for quantitative chemical
analysis, quality assurance. Extraction methods such as
liquid-liquid extraction, solid phase extraction, super-critical
fluid extraction and accelerated solvent extraction. Cleanup and
fractionation methods. Introduction to Chromatography,
high-pressure liquid chromatography (HPLC), gas chromatography (GC)
and other chromatographic methods. Detector types with focus on
mass spectrometry and hyphenated techniques such as GC-MS and
LC-MS. Introduction to spectroscopic methods (UV-VIS, IR, X-ray,
atomic absorption spectroscopy (AAS) and inductive coupled plasma
mass spectrometry). Introduction to data processing, errors in
chemical analyses, statistical analyses (including chemometrics)
and data presentation. Method development, evaluation, validation
and QA/QC measures.
Compulsory laboratory exercises comprise projects which involve sampling, extraction and cleanup, methods of analysis, data processing and data evaluation.
The course objective is to introduce the participants to modern
instrumental techniques and analytical approaches within
environmental- and soil chemistry, food chemistry and plant
After completing the course the student should be able to:
Describe the theory of sampling, sample preparation and sample preparation techniques
Refer to the chemical theory behind the use of modern instrumental techniques for quantitative chemical analysis
Describe how to identify unknown compounds by mass spectrometry and to measure their concentrations in environmental and food samples
Develop and apply methods for separating chemical compounds in mixtures using chromatography
Perform quantitative chemical analysis of organic compounds and metals
Apply solid data processing and evaluation of analytical data
Develop, validate and apply analytical methods in different field of research
Evaluate and discuss analytical chemical data from the literature.
Do problem solving in analytical chemistry
Daniel C. Harris: Quantitative Chemical Analysis
Compendium for laboratory exercises, handouts and electronic resources.
Details will be announced on Absalon.
Theoretical exercises: These exercises will train the students to carry out calculations on the data produced from different instrumental techniques including statistical analyses, reporting and QA/QC.
Laboratory exercises: Laboratory exercises represent the heart of the course. Here, the participants train the different instrumental techniques and get used to analytical work in the laboratory. The laboratory exercises comprise 6 compulsory themes. Theoretical and laboratory exercises are performed by groups of 2 or 3 students. A 1-day excursion to a larger accredited laboratory is included in the course.
- Practical exercises
- Theory exercises
- 7,5 ECTS
- Type of assessment
- Written examination, 3 hours under invigilationPractical oral examination, 20 minThe oral examination will focus on practical aspects of analytical chemistry on the basis of the laboratory exercises. The final grade is based on the written exam (app. 2/3) and the oral examination of practical aspects (app. 1/3).
- Exam registration requirements
Minimum 75% of the reports from the laboratory exercises need to be accepted by the course teacher before final examination
- All aids allowed
- Marking scale
- 7-point grading scale
- Censorship form
- No external censorship
One internal examiner
As the ordinary exam. It is not possible to use either the oral or the written part of the ordinary exam.
If 10 or fewer register for the reexamination the examination form will be oral, 30 min. 40 min preparation (20 min for preparing a given assignment and 20 min for preparing 2 questions in curriculum). All aids allowed exept access to internet.
There can not be dispensated for the requirement of laboratory exercises, and students who do not fullfil the requirement has to follow the course the following study year.
Criteria for exam assesment
See learning outcome